4-Hydroxyoestradiol triacetate is easily prepared from the 4-acetoxymercurio derivative of oestradiol by using lead tetra-acetate in a metal–metal exchange reaction to introduce the oxygen substituent at C-4.
D. N. Kirk and C. J. Slade, J. Chem. Soc., Chem. Commun., 1982, 563 DOI: 10.1039/C39820000563
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