By using i.r. and pulse-dynamic measurements, it has been proved that the rate-determining step in the methanation of CO on a Pd/Al2O3 catalyst is the dissociation of the C–O bond of the adsorbed CO species while the hydrogenation of surface carbon species proceeds rapidly.
H. Niizuma, T. Mori, A. Miyamoto, T. Hattori, H. Masuda, H. Imai and Y. Murakami, J. Chem. Soc., Chem. Commun., 1982, 562 DOI: 10.1039/C39820000562
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