RSC Advances  

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Separation science articles published in the last 6 months

28 items - Showing page 1 of 2
Open Access Paper

Preparation of imidazole-modified paper membrane for selective extraction of gallic acid and its structural and functional analogues from Pomegranate Peel

This work offers a novel approach to preparing a readily synthesized extraction membrane capable of isolating compounds with similar structures and pharmaceutical effects from natural products.

Graphical abstract: Preparation of imidazole-modified paper membrane for selective extraction of gallic acid and its structural and functional analogues from Pomegranate Peel
Open Access Paper

Dispersive micro solid phase extraction of glibenclamide from plasma, urine, and wastewater using a magnetic molecularly imprinted polymer followed by its determination by a high-performance liquid chromatography-photodiode array detector

The present study describes the development of a simple and selective analytical method for dispersive micro solid phase extraction and determination of glibenclamide (GLB) using magnetic molecularly imprinted polymer (MMIP) as a sorbent.

Graphical abstract: Dispersive micro solid phase extraction of glibenclamide from plasma, urine, and wastewater using a magnetic molecularly imprinted polymer followed by its determination by a high-performance liquid chromatography-photodiode array detector
Open Access Review Article

Skin emitted volatiles analysis for noninvasive diagnosis: the current advances in sample preparation techniques for biomedical application

Analytical technique for monitoring skin-emitted metabolites to diagnose diseases.

Graphical abstract: Skin emitted volatiles analysis for noninvasive diagnosis: the current advances in sample preparation techniques for biomedical application
From the themed collection: 2024 Reviews in RSC Advances
Open Access Paper

Enhanced molecular recognition with longer chain crosslinkers in molecularly imprinted polymers for an efficient separation of TR active substances

We report the effects of the crosslinker length on the molecular recognition for the preparation of molecularly imprinted polymers.

Graphical abstract: Enhanced molecular recognition with longer chain crosslinkers in molecularly imprinted polymers for an efficient separation of TR active substances
Open Access Paper

Investigation of bioactive components responsible for the antibacterial and anti-biofilm activities of Caroxylon volkensii by LC-QTOF-MS/MS analysis and molecular docking

Metabolomic profiling of Caroxylon volkensii by LC-QTOF-MS/MS and investigating the components responsible for its antibacterial and anti-biofilm activities using molecular docking.

Graphical abstract: Investigation of bioactive components responsible for the antibacterial and anti-biofilm activities of Caroxylon volkensii by LC-QTOF-MS/MS analysis and molecular docking
From the themed collection: 2024 RSC Advances Popular Advances Collection
Open Access Paper

LC-MS/DIA-based strategy for comprehensive flavonoid profiling: an Ocotea spp. applicability case

A user-friendly LC-MS data-independent acquisition-based strategy using open software for access to the flavonoid content of complex mixtures.

Graphical abstract: LC-MS/DIA-based strategy for comprehensive flavonoid profiling: an Ocotea spp. applicability case
Open Access Review Article

Electrochemical sensing of B-complex vitamins: current challenges and future prospects with microfluidic integration

Vitamins are crucial micronutrients found in limited quantities in food, living organisms, and soil.

Graphical abstract: Electrochemical sensing of B-complex vitamins: current challenges and future prospects with microfluidic integration
From the themed collection: 2024 Reviews in RSC Advances
Open Access Paper

Quantification of the composition of pyrolysis oils of complex plastic waste by gas chromatography coupled with mass spectrometer detector

Waste valorisation through pyrolysis generates solid, liquid and gaseous fractions that need to be deeply characterised in order to try to recover secondary raw materials or chemicals.

Graphical abstract: Quantification of the composition of pyrolysis oils of complex plastic waste by gas chromatography coupled with mass spectrometer detector
Open Access Paper

Developing a novel magnetic organic polymer for selective extraction and determination of 16 macrolides in water and honey samples

A novel magnetic organic polymer Fe3O4@SiO2@Tb–PDAN was designed and synthesized, which was used as an adsorbent for magnetic solid-phase extraction (MSPE) for the determination of 16 MALs.

Graphical abstract: Developing a novel magnetic organic polymer for selective extraction and determination of 16 macrolides in water and honey samples
Open Access Paper

Effective extraction and determination of 24 quinolones in water and egg samples using a novel magnetic covalent organic framework combined with UPLC-MS/MS

We designed and fabricated a novel functionalized magnetic covalent organic framework as a magnetic solid-phase extraction (MSPE) absorbent for the determination of 24 quinolones.

Graphical abstract: Effective extraction and determination of 24 quinolones in water and egg samples using a novel magnetic covalent organic framework combined with UPLC-MS/MS
Open Access Paper

Fabrication of a surface molecularly imprinted polymer membrane based on a single template and its application in the separation and extraction of phenytoin, phenobarbital and lamotrigine

A molecularly imprinted polymer membrane (MIPM) was prepared using PVDF as the support and phenytoin (PHT) as a single template. The results indicated that the MIPMs can be used to extract PHT, phenobarbital, and lamotrigine in different matrices.

Graphical abstract: Fabrication of a surface molecularly imprinted polymer membrane based on a single template and its application in the separation and extraction of phenytoin, phenobarbital and lamotrigine
Open Access Paper

A facile on–off fluorescence approach for fluvoxamine determination in pharmaceutical tablets; application to content uniformity testing

Ion pair complex formation between fluvoxamine and erythrosine B dye quench the fluorescence of the dye in a concentration dependent profile.

Graphical abstract: A facile on–off fluorescence approach for fluvoxamine determination in pharmaceutical tablets; application to content uniformity testing
Open Access Paper

Surfactant modified coconut husk fiber as a green alternative sorbent for micro-solid phase extraction of triazole fungicides at trace level in environmental water, soybean milk, fruit juice and alcoholic beverage samples

Schematic diagram of the micro solid phase extraction (μ-SPE) procedure prior to HPLC analysis.

Graphical abstract: Surfactant modified coconut husk fiber as a green alternative sorbent for micro-solid phase extraction of triazole fungicides at trace level in environmental water, soybean milk, fruit juice and alcoholic beverage samples
Open Access Review Article

Recent reports on the sensing strategy and the On-site detection of illegal drugs

In this review, works on the on-site detection of illegal drugs in recent years are summarised and discussed, most of which were published within the past five years.

Graphical abstract: Recent reports on the sensing strategy and the On-site detection of illegal drugs
From the themed collection: 2024 Reviews in RSC Advances
Open Access Paper

Protection against myocardial ischemia/reperfusion injury in mice by 3-caffeoylquinic acid isomers isolated from Saxifraga tangutica

S. tangutica extract was obtained by medium-pressure liquid chromatography and its activity studied using HPLC-DPPH screening.

Graphical abstract: Protection against myocardial ischemia/reperfusion injury in mice by 3-caffeoylquinic acid isomers isolated from Saxifraga tangutica
Open Access Paper

HPLC-FLD determination of aflatoxins M1 and M2 in raw cow milk samples using in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method

An in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method was employed for the extraction of aflatoxins from cow milk samples prior to their quantification with HPLC equipped with a fluorescence detector.

Graphical abstract: HPLC-FLD determination of aflatoxins M1 and M2 in raw cow milk samples using in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method
Open Access Paper

A simple and reliable QSPR model for prediction of chromatography retention indices of volatile organic compounds in peppers

A simple and reliable QSPR model for the retention indices (RIs) of 273 identified volatile organic compounds (VOCs) of different types of pepper was developed with CORAL software. The proposed theoretical model is applied to estimate the retention indices (RIs) of new VOCs.

Graphical abstract: A simple and reliable QSPR model for prediction of chromatography retention indices of volatile organic compounds in peppers
Open Access Paper

New sorbent-based hydrophobic alginic acid derivatives for fat removal in multi-pesticide residues: analysis of a fatty food sample

Hydrophobic alginic acid derivatives were synthesized with eco-friendly ultrasoundassisted esterification using various aliphatic hydrocarbon chains for fat removal in an analysis of multi-pesticide residues in a fatty food sample.

Graphical abstract: New sorbent-based hydrophobic alginic acid derivatives for fat removal in multi-pesticide residues: analysis of a fatty food sample
Open Access Paper

Determination of phenolic compounds in water using a multivariate statistical analysis method combined with three-dimensional fluorescence spectroscopy

Phenolic compounds are toxic chemical pollutants present in water.

Graphical abstract: Determination of phenolic compounds in water using a multivariate statistical analysis method combined with three-dimensional fluorescence spectroscopy
Open Access Paper

Solute-particle separation in microfluidics enhanced by symmetrical convection

The utilization of microfluidic technology for miniaturized and efficient particle sorting holds significant importance in fields such as biology, chemistry, and healthcare.

Graphical abstract: Solute-particle separation in microfluidics enhanced by symmetrical convection
Open Access Paper

Advances in the characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples by GC-QToF-MS

A new analytical method based on GC-QToF-MS is proposed for the enhanced characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples. New insights into the use of mastic in ancient Egypt are provided.

Graphical abstract: Advances in the characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples by GC-QToF-MS
Open Access Paper

Preparation of novel S-allyl cysteine chitosan based nanoparticles for use in ischemic brain treatment

Enhancing the brain bioavailability of S-allyl-L-cysteine (SC) by developing novel S-allyl-L-cysteine chitosan nanoparticles and examining the quantity of SC by developing a novel method of ultra-high performance liquid chromatography-tandem mass spectrometry in ischemic rat brain treatment.

Graphical abstract: Preparation of novel S-allyl cysteine chitosan based nanoparticles for use in ischemic brain treatment
Open Access Paper

Post-synthetic modified luminescent metal–organic framework for the detection of berberine hydrochloride in a traditional Chinese herb

The fluorescence sensor UiO-66-PSM was prepared by post-synthetic modification. Fluorescence properties of UiO-66-PSM confirmed that the prepared sensor can be applied to the detection of berberine hydrochloride the in traditional Chinese herb Coptis.

Graphical abstract: Post-synthetic modified luminescent metal–organic framework for the detection of berberine hydrochloride in a traditional Chinese herb
Open Access Paper

Tannic acid promotes the activation of persulfate with Fe(II) for highly efficient trichloroethylene removal

Due to the Fe-TA chelation and the reducibility of tannic acid, the concentration of Fe(II) was effectively regulated and slowly released during the removal process to activate persulfate for continuously releasing reactive species.

Graphical abstract: Tannic acid promotes the activation of persulfate with Fe(ii) for highly efficient trichloroethylene removal
Open Access Paper

A novel LC-MS/MS method combined with derivatization for simultaneous quantification of vitamin D metabolites in human serum with diabetes as well as hyperlipidemia

A novel LC-MS/MS method combined with liquid–liquid extraction and derivatization was developed to analyze vitamin D metabolites and applied to the determination of the vitamin D metabolites in human serum with diabetes as well as hyperlipidemia.

Graphical abstract: A novel LC-MS/MS method combined with derivatization for simultaneous quantification of vitamin D metabolites in human serum with diabetes as well as hyperlipidemia
28 items - Showing page 1 of 2

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