RSC Advances
Separation science articles published in the last
6 months
Preparation of imidazole-modified paper membrane for selective extraction of gallic acid and its structural and functional analogues from Pomegranate Peel
This work offers a novel approach to preparing a readily synthesized extraction membrane capable of isolating compounds with similar structures and pharmaceutical effects from natural products.
RSC Adv., 2024,14, 14202-14213
https://doi.org/10.1039/D3RA08576G
Dispersive micro solid phase extraction of glibenclamide from plasma, urine, and wastewater using a magnetic molecularly imprinted polymer followed by its determination by a high-performance liquid chromatography-photodiode array detector
The present study describes the development of a simple and selective analytical method for dispersive micro solid phase extraction and determination of glibenclamide (GLB) using magnetic molecularly imprinted polymer (MMIP) as a sorbent.
RSC Adv., 2024,14, 13168-13179
https://doi.org/10.1039/D4RA00452C
Skin emitted volatiles analysis for noninvasive diagnosis: the current advances in sample preparation techniques for biomedical application
Analytical technique for monitoring skin-emitted metabolites to diagnose diseases.
RSC Adv., 2024,14, 12009-12020
https://doi.org/10.1039/D4RA01579G
Enhanced molecular recognition with longer chain crosslinkers in molecularly imprinted polymers for an efficient separation of TR active substances
We report the effects of the crosslinker length on the molecular recognition for the preparation of molecularly imprinted polymers.
RSC Adv., 2024,14, 12021-12029
https://doi.org/10.1039/D3RA08854E
Investigation of bioactive components responsible for the antibacterial and anti-biofilm activities of Caroxylon volkensii by LC-QTOF-MS/MS analysis and molecular docking
Metabolomic profiling of Caroxylon volkensii by LC-QTOF-MS/MS and investigating the components responsible for its antibacterial and anti-biofilm activities using molecular docking.
RSC Adv., 2024,14, 11388-11399
https://doi.org/10.1039/D4RA01646G
LC-MS/DIA-based strategy for comprehensive flavonoid profiling: an Ocotea spp. applicability case
A user-friendly LC-MS data-independent acquisition-based strategy using open software for access to the flavonoid content of complex mixtures.
RSC Adv., 2024,14, 10481-10498
https://doi.org/10.1039/D4RA01384K
Electrochemical sensing of B-complex vitamins: current challenges and future prospects with microfluidic integration
Vitamins are crucial micronutrients found in limited quantities in food, living organisms, and soil.
RSC Adv., 2024,14, 10331-10347
https://doi.org/10.1039/D4RA00555D
Quantification of the composition of pyrolysis oils of complex plastic waste by gas chromatography coupled with mass spectrometer detector
Waste valorisation through pyrolysis generates solid, liquid and gaseous fractions that need to be deeply characterised in order to try to recover secondary raw materials or chemicals.
RSC Adv., 2024,14, 9892-9911
https://doi.org/10.1039/D4RA00226A
Developing a novel magnetic organic polymer for selective extraction and determination of 16 macrolides in water and honey samples
A novel magnetic organic polymer Fe3O4@SiO2@Tb–PDAN was designed and synthesized, which was used as an adsorbent for magnetic solid-phase extraction (MSPE) for the determination of 16 MALs.
RSC Adv., 2024,14, 8726-8734
https://doi.org/10.1039/D4RA00496E
Effective extraction and determination of 24 quinolones in water and egg samples using a novel magnetic covalent organic framework combined with UPLC-MS/MS
We designed and fabricated a novel functionalized magnetic covalent organic framework as a magnetic solid-phase extraction (MSPE) absorbent for the determination of 24 quinolones.
RSC Adv., 2024,14, 8303-8312
https://doi.org/10.1039/D4RA00247D
Fabrication of a surface molecularly imprinted polymer membrane based on a single template and its application in the separation and extraction of phenytoin, phenobarbital and lamotrigine
A molecularly imprinted polymer membrane (MIPM) was prepared using PVDF as the support and phenytoin (PHT) as a single template. The results indicated that the MIPMs can be used to extract PHT, phenobarbital, and lamotrigine in different matrices.
RSC Adv., 2024,14, 8353-8365
https://doi.org/10.1039/D4RA00294F
A facile on–off fluorescence approach for fluvoxamine determination in pharmaceutical tablets; application to content uniformity testing
Ion pair complex formation between fluvoxamine and erythrosine B dye quench the fluorescence of the dye in a concentration dependent profile.
RSC Adv., 2024,14, 8283-8292
https://doi.org/10.1039/D3RA08257A
Surfactant modified coconut husk fiber as a green alternative sorbent for micro-solid phase extraction of triazole fungicides at trace level in environmental water, soybean milk, fruit juice and alcoholic beverage samples
Schematic diagram of the micro solid phase extraction (μ-SPE) procedure prior to HPLC analysis.
RSC Adv., 2024,14, 7290-7302
https://doi.org/10.1039/D3RA07506K
Recent reports on the sensing strategy and the On-site detection of illegal drugs
In this review, works on the on-site detection of illegal drugs in recent years are summarised and discussed, most of which were published within the past five years.
RSC Adv., 2024,14, 6917-6929
https://doi.org/10.1039/D3RA06931A
Protection against myocardial ischemia/reperfusion injury in mice by 3-caffeoylquinic acid isomers isolated from Saxifraga tangutica
S. tangutica extract was obtained by medium-pressure liquid chromatography and its activity studied using HPLC-DPPH screening.
RSC Adv., 2024,14, 6642-6655
https://doi.org/10.1039/D4RA00046C
HPLC-FLD determination of aflatoxins M1 and M2 in raw cow milk samples using in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method
An in-syringe gas-controlled density tunable solidification of a floating organic droplet-based dispersive liquid–liquid microextraction method was employed for the extraction of aflatoxins from cow milk samples prior to their quantification with HPLC equipped with a fluorescence detector.
RSC Adv., 2024,14, 5077-5084
https://doi.org/10.1039/D3RA04149B
A simple and reliable QSPR model for prediction of chromatography retention indices of volatile organic compounds in peppers
A simple and reliable QSPR model for the retention indices (RIs) of 273 identified volatile organic compounds (VOCs) of different types of pepper was developed with CORAL software. The proposed theoretical model is applied to estimate the retention indices (RIs) of new VOCs.
RSC Adv., 2024,14, 3186-3201
https://doi.org/10.1039/D3RA07960K
New sorbent-based hydrophobic alginic acid derivatives for fat removal in multi-pesticide residues: analysis of a fatty food sample
Hydrophobic alginic acid derivatives were synthesized with eco-friendly ultrasoundassisted esterification using various aliphatic hydrocarbon chains for fat removal in an analysis of multi-pesticide residues in a fatty food sample.
RSC Adv., 2024,14, 2491-2503
https://doi.org/10.1039/D3RA07442K
Determination of phenolic compounds in water using a multivariate statistical analysis method combined with three-dimensional fluorescence spectroscopy
Phenolic compounds are toxic chemical pollutants present in water.
RSC Adv., 2024,14, 2235-2242
https://doi.org/10.1039/D3RA06917F
Solute-particle separation in microfluidics enhanced by symmetrical convection
The utilization of microfluidic technology for miniaturized and efficient particle sorting holds significant importance in fields such as biology, chemistry, and healthcare.
RSC Adv., 2024,14, 1729-1740
https://doi.org/10.1039/D3RA07285A
Advances in the characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples by GC-QToF-MS
A new analytical method based on GC-QToF-MS is proposed for the enhanced characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples. New insights into the use of mastic in ancient Egypt are provided.
RSC Adv., 2024,14, 836-854
https://doi.org/10.1039/D3RA06651G
Preparation of novel S-allyl cysteine chitosan based nanoparticles for use in ischemic brain treatment
Enhancing the brain bioavailability of S-allyl-L-cysteine (SC) by developing novel S-allyl-L-cysteine chitosan nanoparticles and examining the quantity of SC by developing a novel method of ultra-high performance liquid chromatography-tandem mass spectrometry in ischemic rat brain treatment.
RSC Adv., 2024,14, 160-180
https://doi.org/10.1039/D3RA05933B
Post-synthetic modified luminescent metal–organic framework for the detection of berberine hydrochloride in a traditional Chinese herb
The fluorescence sensor UiO-66-PSM was prepared by post-synthetic modification. Fluorescence properties of UiO-66-PSM confirmed that the prepared sensor can be applied to the detection of berberine hydrochloride the in traditional Chinese herb Coptis.
RSC Adv., 2024,14, 602-607
https://doi.org/10.1039/D3RA07054A
Tannic acid promotes the activation of persulfate with Fe(II) for highly efficient trichloroethylene removal
Due to the Fe-TA chelation and the reducibility of tannic acid, the concentration of Fe(II) was effectively regulated and slowly released during the removal process to activate persulfate for continuously releasing reactive species.
RSC Adv., 2023,13, 34371-34377
https://doi.org/10.1039/D3RA06004G
A novel LC-MS/MS method combined with derivatization for simultaneous quantification of vitamin D metabolites in human serum with diabetes as well as hyperlipidemia
A novel LC-MS/MS method combined with liquid–liquid extraction and derivatization was developed to analyze vitamin D metabolites and applied to the determination of the vitamin D metabolites in human serum with diabetes as well as hyperlipidemia.
RSC Adv., 2023,13, 34157-34166
https://doi.org/10.1039/D3RA05700C
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