SCHEDULED MAINTENANCE
Reduction of (Pri2N)2PCl with LiAIH4 in diethyl ether gives (Pri2N)2,PH; reaction of Pri2NPCl2, with Mg in boiling tetrahydrofuran gives either the cyclotetraphosphine (Pri2N)4P4 or the 1,2-dichlorobiphosphine Pri2NP(Cl)–P(Cl)NPri2 depending upon the Mg:Pri2NPCl2 mole ratio.
R. B. King, N. D. Sadanani and P. M. Sundaram, J. Chem. Soc., Chem. Commun., 1983, 477 DOI: 10.1039/C39830000477
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