Saturated and unsaturated aldehydes react with t-butoxyl radicals in fluid solution to show strong well resolved e.s.r. spectra of the corresponding σ-acyl radicals with the same conformations as the parent aldehydes.
A. G. Davies and R. Sutcliffe, J. Chem. Soc., Chem. Commun., 1979, 473 DOI: 10.1039/C39790000473
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