Steffen V. F.
Hansen
ab,
Zoe E.
Wilson
a,
Trond
Ulven
*b and
Steven V.
Ley
*a
aDepartment of Chemistry, University of Cambridge, Lensfield Road, Cambridge, CB2 1EW, UK, svl1000@cam.ac.uk
bDepartment of Physics, Chemistry and Pharmacy, University of Southern Denmark, Campusvej 55, 5230 Odense M, Denmark. E-mail: ulven@sdu.dk
First published on 11th April 2016
Correction for ‘Controlled generation and use of CO in flow’ by Steffen V. F. Hansen et al., React. Chem. Eng., 2016, DOI: 10.1039/c6re00020g.
# | Iodidea | Product | Yieldb | # | Iodidea | Product | Yieldb | # | Iodidea | Product | Yieldb |
---|---|---|---|---|---|---|---|---|---|---|---|
a All reactions were carried out on 0.5 mmol scale apart from #8 which was run continuously on 8 mmol scale (320 minutes).
b Isolated yield.
c Methanol was used as the solvent for pump 3, the reaction coil was heated to 25 °C and sample loop filled with iodide 5 (0.1 M), Pd(OAc)2 (0.01 eq.), XantPhos (0.012 eq.), NEt3 (1.5 eq.), H2NNH2 (0.3 eq.) and THF/MeOH (1![]() ![]() |
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1c |
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71% | 4 |
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74% | 7a |
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79% |
2 |
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97% | 5 |
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78% | 8d |
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96% (1.47 g) |
3 |
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99% | 6 |
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78% |
The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.
This journal is © The Royal Society of Chemistry 2016 |