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Correction: Controlled generation and use of CO in flow

Steffen V. F. Hansen ab, Zoe E. Wilson a, Trond Ulven *b and Steven V. Ley *a
aDepartment of Chemistry, University of Cambridge, Lensfield Road, Cambridge, CB2 1EW, UK, svl1000@cam.ac.uk
bDepartment of Physics, Chemistry and Pharmacy, University of Southern Denmark, Campusvej 55, 5230 Odense M, Denmark. E-mail: ulven@sdu.dk

Received 5th April 2016 , Accepted 5th April 2016

First published on 11th April 2016


Abstract

Correction for ‘Controlled generation and use of CO in flow’ by Steffen V. F. Hansen et al., React. Chem. Eng., 2016, DOI: 10.1039/c6re00020g.


In the above article, Table 3 did not include a yield for entry 5. The correct information can be found in the new version of Table 3 below.
Table 3 Alkoxycarbonylation of vinyl and aryl iodides with modified set up

image file: c6re90010k-u1.tif

# Iodidea Product Yieldb # Iodidea Product Yieldb # Iodidea Product Yieldb
a All reactions were carried out on 0.5 mmol scale apart from #8 which was run continuously on 8 mmol scale (320 minutes). b Isolated yield. c Methanol was used as the solvent for pump 3, the reaction coil was heated to 25 °C and sample loop filled with iodide 5 (0.1 M), Pd(OAc)2 (0.01 eq.), XantPhos (0.012 eq.), NEt3 (1.5 eq.), H2NNH2 (0.3 eq.) and THF/MeOH (1[thin space (1/6-em)]:[thin space (1/6-em)]1). d Continuous flow reaction.
1c image file: c6re90010k-u2.tif 5 image file: c6re90010k-u3.tif 6 71% 4 image file: c6re90010k-u4.tif 11 image file: c6re90010k-u5.tif 15 74% 7a image file: c6re90010k-u6.tif 14 image file: c6re90010k-u7.tif 18 79%
2 image file: c6re90010k-u8.tif 7 image file: c6re90010k-u9.tif 9 97% 5 image file: c6re90010k-u10.tif 12 image file: c6re90010k-u11.tif 16 78% 8d image file: c6re90010k-u12.tif 7 image file: c6re90010k-u13.tif 9 96% (1.47 g)
3 image file: c6re90010k-u14.tif 8 image file: c6re90010k-u15.tif 10 99% 6 image file: c6re90010k-u16.tif 13 image file: c6re90010k-u17.tif 17 78%


The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.


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