Alkali metal reduction of M2(CO)10 or M(CO)5–(M ![[double bond, length as m-dash]](https://www.rsc.org/images/entities/char_e001.gif)
Mn and Re) in hexamethylphosphoramide provides the first non-cluster binary metal carbonyl trianions, M(CO)43–, which are characterized by their spectral and chemical properties.
J. E. Ellis and R. A. Faltynek, J. Chem. Soc., Chem. Commun., 1975, 966 DOI: 10.1039/C39750000966
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