The first example of an osmium cluster containing µ4-oxo groups, [Os11(µ4-O)(CO)30]1, has been obtained from the vacuum pyrolysis of [Os3H(CO)10(µ-OH)], and has been shown by X-ray crystallography to contain a tri-edge bridged, bicapped trigonal prismatic metal core.
S. L. Ingham, J. Lewis and P. R. Raithby, J. Chem. Soc., Chem. Commun., 1993, 166 DOI: 10.1039/C39930000166
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