Radical cyclizations of the ω-iodoaldehyde (6), ω-iodonitrile (5), and ω-iodo-α,β-unsaturated ester (9) afford approximately 55, 2, and 80% yields, respectively, of cyclohexanofuranoses; these products are readily formed from the ester cyclizations, providing a key intermediate in Collum's synthesis of phyllanthocin.
B. A. Yeung, J. L. M. Contelles and B. Fraser-Reid, J. Chem. Soc., Chem. Commun., 1989, 1160 DOI: 10.1039/C39890001160
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