The title compound has been examined by single-crystal X-ray diffraction and crystallises in the space group P21/c with Z= 4 in a unit cell of dimensions a= 6·12, b= 13·72, c= 13·38 Å, and β= 100·4°. The molecules of SnCl4,2MeCN are cis-octahedral. The i.r. and Raman spectrum of the adducts and its deuterio-analogue are reported and the vibrational assignment discussed.
M. Webster and H. E. Blayden, J. Chem. Soc. A, 1969, 2443 DOI: 10.1039/J19690002443
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