Acetyl heptachlorodialuminate has been prepared from acetyl chloride and aluminium chloride in liquid hydrogen chloride. Conductometric titrations of tetra-alkylammonium chlorides against aluminium chloride in acetyl chloride as a solvent have been carried out and end-points found corresponding to the formation of both heptachlorodialuminate and tetrachloroaluminate ions.
M. E. Peach, V. L. Tracy and T. C. Waddington, J. Chem. Soc. A, 1969, 366 DOI: 10.1039/J19690000366
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