Pyrolysis of phenyl 2,2,2-trideuterioacetate yields phenol with no ortho-deuterium, indicating that the reaction does not involve a concerted sigmatropic rearrangement.
A. C. Barefoot and F. A. Carroll, J. Chem. Soc., Chem. Commun., 1974, 357 DOI: 10.1039/C39740000357
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