The synthesis and cyclic voltammetry data of cage-like molecules incorporating extended tetrathiafulvalenes are reported together with the demonstration that the two crystal modifications (1.289 and 1.311 g cm–3) observed for 2b correspond to two different cis conformers A and B, the most planar form (B) giving the more dense crystal packing.
P. Hascoat, D. Lorcy, A. Robert, K. Boubekeur, P. Batail, R. Carlier and A. Tallec, J. Chem. Soc., Chem. Commun., 1995, 1229 DOI: 10.1039/C39950001229
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