Issue 51, 2024

Elimination of homogeneous broadening in 1H solid-state NMR

Abstract

1H solid-state NMR spectra are plagued by low resolution, necessitating the use of complex pulse sequences or specialized equipment. We introduce a new resolution enhancement method, inspired by super-resolution microscopy, that uses a 2D Hahn-echo experiment to constrain deconvolution. The result is an effective doubling of the MAS frequency.

Graphical abstract: Elimination of homogeneous broadening in 1H solid-state NMR

Article information

Article type
Communication
Submitted
06 mai 2024
Accepted
31 mai 2024
First published
03 juin 2024

Chem. Commun., 2024,60, 6552-6555

Elimination of homogeneous broadening in 1H solid-state NMR

F. A. Perras, Chem. Commun., 2024, 60, 6552 DOI: 10.1039/D4CC02191F

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Social activity

Spotlight

Advertisements