Issue 4, 2020
From the journal:

Dalton Transactions

Facile synthesis of novel lithium β-diketonate glyme adducts: the effect of molecular engineering on the thermal properties†

Nishant Peddagopu, ORCID logo a   Patrizia Rossi, ORCID logo b   Carmela Bonaccorso, ORCID logo c   Ausrine Bartasyte, ORCID logo d   Paola Paoli ORCID logo b  and  Graziella Malandrino ORCID logo *a  

* Corresponding authors

a Dipartimento di Scienze Chimiche, Università di Catania and INSTM UdR Catania, V.le Andrea Doria 6, 95125 Catania, Italy
E-mail: gmalandrino@unict.it

b Dipartimento di Ingegneria Industriale, Università di Firenze, Via Santa Marta 3, 50136 Firenze, Italy

c Dipartimento di Scienze Chimiche, Università di Catania, V.le Andrea Doria 6, 95125 Catania, Italy

d FEMTO-ST Institute, University of Bourgogne Franche-Comté CNRS UMR 6174, 26 Rue de l'Epitaphe, F-25030 Besançon, France

Abstract

Novel adducts of lithium hexafluoroacetylacetonato {Li(hfa)} with polyethers (monoglyme = {CH3OCH2CH2OCH3}, diglyme = {CH3O(CH2CH2O)2CH3}, triglyme = {CH3O(CH2CH2O)3CH3} and tetraglyme {CH3O(CH2CH2O)4CH3} have been synthesized through a single step reaction and characterized by FT-IR spectroscopy, 1H, and 13C NMR, single crystal X-ray diffraction studies along with thermal analysis.

Graphical abstract: Facile synthesis of novel lithium β-diketonate glyme adducts: the effect of molecular engineering on the thermal properties

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Article information

DOI
https://doi.org/10.1039/C9DT04732H
Article type
Communication
Submitted
12 Dec 2019
Accepted
03 Jan 2020
First published
03 Jan 2020

Dalton Trans., 2020,49, 1002-1006

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Facile synthesis of novel lithium β-diketonate glyme adducts: the effect of molecular engineering on the thermal properties

N. Peddagopu, P. Rossi, C. Bonaccorso, A. Bartasyte, P. Paoli and G. Malandrino, Dalton Trans., 2020, 49, 1002 DOI: 10.1039/C9DT04732H

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