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Issue 6, 2019
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SO2F2 mediated dehydrative cross-coupling of alcohols with electron-deficient olefins in DMSO using a Pd-catalyst: one-pot transformation of alcohols into 1,3-dienes

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Abstract

A Pd-catalyzed, SO2F2 mediated dehydrative cross-coupling reaction of alcohols with acrylates for the construction of 1,3-dienes was developed. The reaction proceeded efficiently under mild conditions and tolerated a wide range of functional groups. This new reaction provided a strategically distinct approach to highly valuable 1,3-diene derivatives from readily available and abundant alcohols.

Graphical abstract: SO2F2 mediated dehydrative cross-coupling of alcohols with electron-deficient olefins in DMSO using a Pd-catalyst: one-pot transformation of alcohols into 1,3-dienes

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Article information


Submitted
21 Dec 2018
Accepted
30 Jan 2019
First published
02 Feb 2019

Org. Chem. Front., 2019,6, 796-800
Article type
Research Article

SO2F2 mediated dehydrative cross-coupling of alcohols with electron-deficient olefins in DMSO using a Pd-catalyst: one-pot transformation of alcohols into 1,3-dienes

R. Lekkala, R. Lekkala, B. Moku and H. Qin, Org. Chem. Front., 2019, 6, 796
DOI: 10.1039/C8QO01388H

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