Zirconia-supported rhenium oxide as an efficient catalyst for the synthesis of biomass-based adipic acid ester

Jinchi Lin; Haiyan Song; Xiaoru Shen; Binju Wang; Shunji Xie; Weiping Deng; Deyin Wu; Qinghong Zhang; Ye Wang

doi:10.1039/C9CC05413H

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Zirconia-supported rhenium oxide as an efficient catalyst for the synthesis of biomass-based adipic acid ester†

Jinchi Lin,^a Haiyan Song,^a Xiaoru Shen,^a Binju Wang,^a Shunji Xie,

^a Weiping Deng,

*^a Deyin Wu,

^a Qinghong Zhang^a and Ye Wang

*^a

Author affiliations

* Corresponding authors

^a State Key Laboratory of Physical Chemistry of Solid Surfaces, Collaborative Innovation Center of Chemistry for Energy Materials, National Engineering Laboratory for Green Chemical Productions of Alcohols, Ethers and Esters, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China
E-mail: dengwp@xmu.edu.cn, wangye@xmu.edu.cn

Abstract

Synthesis of adipic acid, a key monomer of nylon-66 and polyurethane, from biomass is highly attractive for establishing green and sustainable chemical processes. Here, we report that zirconia-supported rhenium oxide (ReO_x/ZrO₂) efficiently catalyses the deoxydehydration of cellulose-derived D-glucaric acid, offering adipic acid ester with a yield of 82% by combining with a Pd/C catalyst in subsequent reactions.

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Article information

DOI: https://doi.org/10.1039/C9CC05413H
Article type: Communication
Submitted: 14 Jul 2019
Accepted: 13 Aug 2019
First published: 13 Aug 2019

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Chem. Commun., 2019,55, 11017-11020

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Zirconia-supported rhenium oxide as an efficient catalyst for the synthesis of biomass-based adipic acid ester

J. Lin, H. Song, X. Shen, B. Wang, S. Xie, W. Deng, D. Wu, Q. Zhang and Y. Wang, Chem. Commun., 2019, 55, 11017 DOI: 10.1039/C9CC05413H

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Chemical Communications

Zirconia-supported rhenium oxide as an efficient catalyst for the synthesis of biomass-based adipic acid ester†

Abstract

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Zirconia-supported rhenium oxide as an efficient catalyst for the synthesis of biomass-based adipic acid ester

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