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Issue 12, 2017
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Synthesis of cyclohexylidenehydrazine-fused polycyclics via a photocatalytic radical cascade reaction of 2-ethynylaldehyde hydrazones

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Abstract

A general and efficient visible-light photoredox-catalyzed cascade annulation of 2-ethynylaldehyde hydrazones with α-bromo-carbonyls for the synthesis of various cyclohexylidene-hydrazine-fused polycyclic compounds is described. This protocol is characterized by a broad substrate scope, mild conditions and amenability to gram-scale synthesis.

Graphical abstract: Synthesis of cyclohexylidenehydrazine-fused polycyclics via a photocatalytic radical cascade reaction of 2-ethynylaldehyde hydrazones

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Publication details

The article was received on 12 Dec 2016, accepted on 18 Jan 2017 and first published on 18 Jan 2017


Article type: Communication
DOI: 10.1039/C6CC09863K
Citation: Chem. Commun., 2017,53, 2036-2039

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    Synthesis of cyclohexylidenehydrazine-fused polycyclics via a photocatalytic radical cascade reaction of 2-ethynylaldehyde hydrazones

    N. Zhou, J. Liu, Z. Yan, Z. Wu, H. Zhang, W. Li and C. Zhu, Chem. Commun., 2017, 53, 2036
    DOI: 10.1039/C6CC09863K

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