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Issue 1, 2017
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Chemically synthesized and cross-linked PDMS as versatile alignment medium for organic compounds

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Abstract

A useful procedure for the preparation of chemically synthesized and cross-linked polydimethylsiloxane (PDMS) gels is presented, which does not require β-irradiation for cross-linking. NMR spectra of high quality are obtained, such that even mixtures of compounds exhibiting similar NMR spectra like interconverting stereoisomers can be investigated in the residual dipolar coupling (RDC) approach of organic structure determination.

Graphical abstract: Chemically synthesized and cross-linked PDMS as versatile alignment medium for organic compounds

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Publication details

The article was received on 01 Nov 2016, accepted on 23 Nov 2016 and first published on 23 Nov 2016


Article type: Communication
DOI: 10.1039/C6CC08762K
Chem. Commun., 2017,53, 95-98

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    Chemically synthesized and cross-linked PDMS as versatile alignment medium for organic compounds

    Y. E. Moskalenko, V. Bagutski and C. M. Thiele, Chem. Commun., 2017, 53, 95
    DOI: 10.1039/C6CC08762K

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