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Issue 55, 2016
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Determining carbon–carbon connectivities in natural abundance organic powders using dipolar couplings

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Abstract

We present a solid-state NMR methodology capable of investigating the carbon skeleton of natural abundance organic powders. The methodology is based on the 13C–13C dipolar coupling interaction and allows carbon–carbon connectivities to be unambiguously established for a wide range of organic solids. This methodology is particularly suitable for disordered solids, such as natural or synthetic macromolecules, which cannot be studied using conventional diffraction or NMR techniques.

Graphical abstract: Determining carbon–carbon connectivities in natural abundance organic powders using dipolar couplings

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Publication details

The article was received on 18 May 2016, accepted on 12 Jun 2016 and first published on 13 Jun 2016


Article type: Communication
DOI: 10.1039/C6CC04202C
Chem. Commun., 2016,52, 8565-8568
  • Open access: Creative Commons BY-NC license
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    Determining carbon–carbon connectivities in natural abundance organic powders using dipolar couplings

    M. Dekhil, G. Mollica, T. T. Bonniot, F. Ziarelli, P. Thureau and S. Viel, Chem. Commun., 2016, 52, 8565
    DOI: 10.1039/C6CC04202C

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