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Issue 2, 2016
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Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

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Abstract

We demonstrate the accessibility of aliphatic 13C side chain chemical shift sets for solid-state NMR despite perdeuteration and fast MAS using isotropic, non-rotor-synchronized 13C–13C mixing. Combined with amide proton detection, we unambiguously and sensitively detect whole side chain to backbone correlations for two proteins using around 1 mg of sample.

Graphical abstract: Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

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The article was received on 01 Sep 2015, accepted on 21 Oct 2015 and first published on 22 Oct 2015


Article type: Communication
DOI: 10.1039/C5CC07345F
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Chem. Commun., 2016,52, 268-271

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    Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

    N. Kulminskaya, S. K. Vasa, K. Giller, S. Becker, A. Kwan, M. Sunde and R. Linser, Chem. Commun., 2016, 52, 268
    DOI: 10.1039/C5CC07345F

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