Jump to main content
Jump to site search

Issue 2, 2016
Previous Article Next Article

Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

Author affiliations

Abstract

We demonstrate the accessibility of aliphatic 13C side chain chemical shift sets for solid-state NMR despite perdeuteration and fast MAS using isotropic, non-rotor-synchronized 13C–13C mixing. Combined with amide proton detection, we unambiguously and sensitively detect whole side chain to backbone correlations for two proteins using around 1 mg of sample.

Graphical abstract: Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

Back to tab navigation

Supplementary files

Article information


Submitted
01 Sep 2015
Accepted
21 Oct 2015
First published
22 Oct 2015

Chem. Commun., 2016,52, 268-271
Article type
Communication
Author version available

Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing

N. Kulminskaya, S. K. Vasa, K. Giller, S. Becker, A. Kwan, M. Sunde and R. Linser, Chem. Commun., 2016, 52, 268
DOI: 10.1039/C5CC07345F

Social activity

Search articles by author

Spotlight

Advertisements