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We found that twinned gold nanoparticles (T-AuNPs) are generated at a high probability by CO treatment of TiO2-supported Au(III) at room temperature. Because of the formation of T-AuNPs, the Au/TiO2 prepared by the CO treatment showed higher catalytic activity for CO oxidation than Au/TiO2 prepared by conventional H2 treatment.

Graphical abstract: Preparation of TiO2-supported twinned gold nanoparticles by CO treatment and their CO oxidation activity

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