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Issue 15, 2014
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Measurements of local chemistry and structure in Ni(O)–YSZ composites during reduction using energy-filtered environmental TEM

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Abstract

Energy-filtered transmission electron microscopy images are acquired during the reduction of a NiO–YSZ composite in H2 up to 600 °C. Temperature-resolved quantitative information about both chemistry and structure is extracted with nm spatial resolution from the data, paving the way for the development of detailed reduction models.

Graphical abstract: Measurements of local chemistry and structure in Ni(O)–YSZ composites during reduction using energy-filtered environmental TEM

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Article information


Submitted
01 Sep 2013
Accepted
09 Dec 2013
First published
09 Dec 2013

Chem. Commun., 2014,50, 1808-1810
Article type
Communication

Measurements of local chemistry and structure in Ni(O)–YSZ composites during reduction using energy-filtered environmental TEM

Q. Jeangros, T. W. Hansen, J. B. Wagner, R. E. Dunin-Borkowski, C. Hébert, J. Van herle and A. Hessler-Wyser, Chem. Commun., 2014, 50, 1808
DOI: 10.1039/C3CC46682E

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