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Two chiral MOFs from the common Zn4O(COO)6 SBUs and the congeners of chiral ligands were synthesized and characterized. The overall structures are differentiated by the ligand dimensions. These MOFs obtained from the flexible enantiopure struts exhibited severe chirality attenuation during the assembly.

Graphical abstract: Chiral porous metal–organic frameworks from chiral building units with different metrics

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