Issue 43, 2007
From the journal:

Chemical Communications

Palladium-catalyzed 1,3-diol fragmentation: synthesis of ω-dienyl aldehydes†‡

Masanari Kimura,a   Masahiko Moria  and  Yoshinao Tamaru*b  

* Corresponding authors

a Graduate School of Science and Technology, Nagasaki University, 1-14 Bunkyo-Machi, Japan

b Department of Applied Chemistry, Faculty of Engineering, Nagasaki University, 1-14 Bunkyo-Machi, Japan
E-mail: tamaru@nagasaki-u.ac.jp

Abstract

2-(1′-Hydroxy-2′-propenyl)cycloalkan-1-ols 1 undergo dehydrative C1–C2 bond cleavage and provide ω-dienyl aldehydes2 under the catalysis of Pd(0) and 9-phenyl-9-BBN.

Graphical abstract: Palladium-catalyzed 1,3-diol fragmentation: synthesis of ω-dienyl aldehydes

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Article information

DOI
https://doi.org/10.1039/B708526E
Article type
Communication
Submitted
05 Jun 2007
Accepted
14 Aug 2007
First published
31 Aug 2007

Chem. Commun., 2007, 4504-4506

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Palladium-catalyzed 1,3-diol fragmentation: synthesis of ω-dienyl aldehydes

M. Kimura, M. Mori and Y. Tamaru, Chem. Commun., 2007, 4504 DOI: 10.1039/B708526E

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