Issue 17, 2004

Abstract

Through the simple expedient of using a mixture of KF and silica as the stationary phase in column chromatography, levels of organotin impurities from tributyltin hydride mediated reductions have been reduced from stoichiometric levels to ∼ 30 ppm.

Graphical abstract: KF–Silica as a stationary phase for the chromatographic removal of tin residues from organic compounds

Supplementary files

Article information

Article type
Communication
Submitted
22 Apr 2004
Accepted
26 May 2004
First published
12 Jul 2004

Chem. Commun., 2004, 1968-1969

KF–Silica as a stationary phase for the chromatographic removal of tin residues from organic compounds

D. C. Harrowven and I. L. Guy, Chem. Commun., 2004, 1968 DOI: 10.1039/B406041E

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