Heating butylamino adducts of diazabis-(1,6);(1,9)-homofullerenes bearing MEM-protected imino bridges with toluene-p-sulfonic acid provides a new route to (C59N)2 in macroscopic amounts and also provides, for the first time, the synthesis and isolation of (C69N)2 and the heterofullerene adducts RC59N and RC69N.
B. Nuber and A. Hirsch, Chem. Commun., 1996, 1421 DOI: 10.1039/CC9960001421
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