The 1-(ω-nitropropyl)- and 1-(ω-nitrobutyl)-6-hydroxytetralins 10 and 16, obtained by new sequences from 6-methoxytetralone, undergo stereospecific intramolecular coupling between phenolate and nitronate functions, to yield the tricyclospirodienones 11, 70%, and 17, 66%.
D. Hobbs-Mallyon and D. A. Whiting, J. Chem. Soc., Chem. Commun., 1991, 899 DOI: 10.1039/C39910000899
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