A 13C chemical-shift powder pattern for ferrocene enclathrated in the deoxycholic acid channel selectively observed by SASS NMR reveals that the included ferrocene molecule is rotating around its five-fold axis; moreover, the axis is rotating on a cone with a half-angle of 18° at ambient temperature.
F. Imashiro, N. Kitazaki, D. Kuwahara, T. Nakai and T. Terao, J. Chem. Soc., Chem. Commun., 1991, 85 DOI: 10.1039/C39910000085
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