The iron-catalysed coupling reaction of three components, perfluoroalkyl iodides, enol ethers and alcohols, in the presence of a base gives directly perfluoroalkyl-substituted acetals in good to excellent yields.
S. Sasaoka, M. Uno, T. Joh, H. Lmazaki and S. Takahashi, J. Chem. Soc., Chem. Commun., 1991, 86 DOI: 10.1039/C39910000086
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