Tricyclic keto diols have been synthesised by a new, three-step annulation procedure in which hydroxyenones, prepared by the coupling of 2-cyclohexen-1-one with aldehydes, are diastereoselectively epoxidised and the syn-epoxides cyclised with tin(IV) chloride.
C. M. Marson, D. W. M. Benzies, A. D. Hobson, H. Adams and N. A. Bailey, J. Chem. Soc., Chem. Commun., 1990, 1516 DOI: 10.1039/C39900001516
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