Irradiation of hypoiodites of steroidal α-oxo tertiary alcohols in the presence of mercury(II) oxide and iodine in benzene gave α-hydroxy ε-lactones and enolic ε-lactone; the mechanism of their formation is discussed on the basis of an 18O labelling study.
H. Suginome, J. B. Wang and G. Satoh, J. Chem. Soc., Perkin Trans. 1, 1989, 1553 DOI: 10.1039/P19890001553
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