Cross-polarization magic-angle-spinning 29Si n.m.r. scanning calorimetry, and X-ray diffraction of well-ordered, as-synthesized samples of the clathrasil dodecasil 3-C (Zeolite ZSM-39) show the presence of three thermally induced phase transitions and indicate an important role for the guest molecules in determining the physical properties of this material.
J. A. Ripmeester, M. A. Desando, Y. P. Handa and J. S. Tse, J. Chem. Soc., Chem. Commun., 1988, 608 DOI: 10.1039/C39880000608
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