Desilylation of the ketene acetals (5) and (9) provides the ene-1,1-diols (6) and (10) which undergo relatively slow ketonisation and are oxidized to stable free radicals in basic solution.
P. O'Neill and A. F. Hegarty, J. Chem. Soc., Chem. Commun., 1987, 744 DOI: 10.1039/C39870000744
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