Electron–optical and related techniques show that both unannealed and annealed samples of Co0.73Fe2.27O4 of colloidal dimensions are highly crystalline and of well-defined morphology: samples annealed at 600 °C have particles of mean diameter ca. 220 Å, with 〈332〉 preferred zones and {022} and {311} preferred faces.
J. Tirado, J. M. Thomas, D. A. Jefferson, G. R. Millward and S. W. Charles, J. Chem. Soc., Chem. Commun., 1987, 365 DOI: 10.1039/C39870000365
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