SCHEDULED MAINTENANCE
The reaction of N2O3 with 2,2,2-trichloroethyl 3-methyl-7β-phenoxyacetamidoceph-3-em-4-carboxylate gives by a new reaction mode, 2,2,2-trichloroethyl 4α-hydroxy-3α-methyl-3β-nitro-7β-phenoxyacetamidocepham-4-carboxylate, the structure and stereochemistry of which were elucidated by 400 MHz n.m.r. and difference nuclear Overhauser enhancement spectroscopy.
M. M. Campbell, B. P. Connarty, J. Kemp and S. J. Ray, J. Chem. Soc., Chem. Commun., 1982, 748 DOI: 10.1039/C39820000748
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