Metal–hydrogen stretching absorptions have been observed in the i.r. spectra of the ions [HRu6(CO)18]– and [DRu6(CO)18]– near 825 and 600 cm–1, respectively, constituting the first reported observation of νMH for an interstitial hydrogen ligand.
I. A. Oxton, S. F. A. Kettle, P. F. Jackson, B. F. G. Johnson and J. Lewis, J. Chem. Soc., Chem. Commun., 1979, 687 DOI: 10.1039/C39790000687
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