Thermal fission and re-formation of the C–N bond in formamide was detected by change of 13C–15N coupled peaks to an uncoupled peak in the 13C n.m.r. spectra.
K. T. Suzuki, H. Yamada and M. Hirobe, J. Chem. Soc., Chem. Commun., 1978, 485 DOI: 10.1039/C39780000485
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