Under u.v. radiation diaryl disulphides (C6H4-p-R)2S2(R = H or Me) yield (C6H3R-o-SC6H4R)2S2, which reacts with a variety of transition metal complexes to provide metallacycles [graphic omitted]C6H4R; one of these [Ru(CO)(SC6H3Me-o-SC6H4Me)(η-C5H5)], has been structurally identified by X-ray diffraction.
S. D. Killops, S. A. R. Knox, G. H. Riding and A. J. Welch, J. Chem. Soc., Chem. Commun., 1978, 486 DOI: 10.1039/C39780000486
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