Benzoylation of monoprotected polymer-bound symmetrical aliphatic diamines at the free amino end and cleavage with trifluoroacetic acid yields the unsymmetrical diamides, CF3CONH[CH2]nNHCOPh, where n= 4, 6, 8, 10, or 12.
D. M. Dixit and C. C. Leznoff, J. Chem. Soc., Chem. Commun., 1977, 798 DOI: 10.1039/C39770000798
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