Reduction of 6-Me3N-6-CB9H11(I) to 6-CB9H12–(II) and hydrolytic degradation of (II) to 4-CB8H14(III), the first monocarbaborane belonging to the arachno-series, are described; structures for these compounds are proposed on the basis of their genesis and n.m.r. spectra.
B. Štíbr, K. Baše, S. Heřmánek and J. Plešek, J. Chem. Soc., Chem. Commun., 1976, 150 DOI: 10.1039/C39760000150
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