Photolysis of o-nitrobenzaldehyde N-acetyl-N-alkylhydrazones gave benzyne via o-nitrosobenzoyl-N-acetyl-N-alkylhydrazides and o-(N-alkyl-N-acetyltriazeno)benzoic acids.
Y. Maki, T. Furuta, M. Kuzuya and M. Suzuki, J. Chem. Soc., Chem. Commun., 1975, 616 DOI: 10.1039/C39750000616
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