Methylene(bis)tetrafluorophosphorane has been prepared by cleavage of the Si–C bond of 1,1,3,3-tetra-methyl-1,3-disilacyclobutane with phosphorus penta-fluoride; it has been characterized by chemical means and by n.m.r. and mass spectroscopy.
W. Althoff, M. Fild, H. Koop and R. Schmutzler, J. Chem. Soc., Chem. Commun., 1975, 468 DOI: 10.1039/C39750000468
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