Thermal rearrangement of α-cyano-α-oxo-epoxides quantitatively affords the corresponding dioxoles, which are formed by initial cleavage between the two carbon atoms of the starting epoxide ring.
A. Robert and B. Moisan, J. Chem. Soc., Chem. Commun., 1972, 337 DOI: 10.1039/C39720000337
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