Total synthesis of (±)-O-methylandrocymbine (II) by photo-Pschorr reaction of 1-(2-amino-3,4,5-trimethoxyphenethyl)-7-benzyloxy-1,2,3,4-tetrahydro-6-methoxy-2-methylisoquinoline (V) is reported.
T. Kametani, M. Koizumi and K. Fukumoto, J. Chem. Soc. D, 1970, 1157 DOI: 10.1039/C29700001157
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