This work demonstrates a stepwise assembly process to prepare [Pd(Pd2L4)]n-type 2D nanosheets using Pd(II) and a stoichiometry-controlled metal–organic cage of Pd2L4 type. A convenient design strategy for dynamic interconversion between cage-based 2D nanosheets and well-defined monomeric cages is achieved.
V. Sivalingam and D. K. Chand, Chem. Commun., 2025, Advance Article , DOI: 10.1039/D4CC06557C
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