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Correction: Method for extraction and analysis of per- and poly-fluoroalkyl substances in contaminated asphalt

Prashant Srivastava *a, Mike Williams a, Jun Du a, Divina Navarro a, Rai Kookana a, Grant Douglas b, Trevor Bastow b, Greg Davis b and Jason K. Kirby a
aCommonwealth Scientific and Industrial Research Organisation (CSIRO), Land and Water, Waite Campus, Urrbrae, South Australia, Australia. E-mail: Prashant.Srivastava@csiro.au
bCommonwealth Scientific and Industrial Research Organisation (CSIRO), Land and Water, Floreat, Western Australia, Australia

Received 15th August 2022 , Accepted 15th August 2022

First published on 25th August 2022


Abstract

Correction for ‘Method for extraction and analysis of per- and poly-fluoroalkyl substances in contaminated asphalt’ by Prashant Srivastava et al., Anal. Methods, 2022, 14, 1678–1689, https://doi.org/10.1039/D2AY00221C.


In the original article, an inadvertent error occurred in the units of PFAS concentration presented in Tables 1 and S1 (ESI). While this has no impact on the methodology described in the paper per se, the units in the tables (Tables 1 and S1) and associated text (pages 1678, 1681, 1683, 1685, 1686 and 1687) should be read as μg kg−1, instead of mg kg−1.

• In Table 1 (page 1681), the unit of concentration of PFOA, PFHxS, PFOS and the sum of PFHxS and PFOS should be μg kg−1, instead of mg kg−1. Therefore, the superscript ‘c’ in Table 1 is redundant, as none of the concentrations exceeds the landfill acceptance criteria of 50 mg kg−1. All discussions referring to Table 1 should have units of μg kg−1 instead of mg kg−1.

• In Table S1 (ESI), the unit of MLOQ should be μg kg−1, instead of mg kg−1.

• The penultimate sentences in the abstract (page 1678) and the first paragraph of the conclusions (page 1687) should have units of μg kg−1 instead of mg kg−1, i.e. (from LOQ to 2135 μg kg−1).

• The final sentence of Section 2.6 (page 1683), text in Section 3.1 (page 1685) and paragraph two of Section 3.3 (page 1686) should have units of μg kg−1 instead of mg kg−1.

The corrected Table 1 is shown below, and the corrected ESI is available – see https://doi.org/10.1039/D2AY90109A.

Table 1 PFOA, PFHxS and PFOS concentrations determined in asphalt cores collected from different locations at an operational airbase in Australia
Location No. Depth (mm) PFOA (μg kg−1) PFHxS (μg kg−1) PFOS (μg kg−1) Sum of PFHxS and PFOS (μg kg−1)
a LOQ = limit of quantitation. b Concentrations without standard deviation had non-detect values for other replicates.
LOQa 0.60 1.00 0.70
Runway apron Core 1 0–50 <LOQ <LOQ <LOQ <LOQ
190–240 <LOQ <LOQ <LOQ <LOQ
Core 2 0–50 <LOQ <LOQ <LOQ <LOQ
180–230 <LOQ <LOQ <LOQ <LOQ
Runway Core 3 0–50 <LOQ <LOQ 1.40 ± 0.30 1.40 ± 0.30
50–80 <LOQ <LOQ 1.39 ± 0.12 1.39 ± 0.12
80–110 <LOQ <LOQ 3.12b 3.12b
110–140 <LOQ <LOQ <LOQ <LOQ
140–170 <LOQ <LOQ <LOQ <LOQ
170–220 <LOQ <LOQ <LOQ <LOQ
220–250 <LOQ <LOQ <LOQ <LOQ
Core 4 0–50 <LOQ 3.10 ± 0.04 9.90 ± 0.40 13.00 ± 0.80
50–70 <LOQ 2.20 ± 0.27 22.00 ± 2.70 24.20 ± 2.97
70–110 0.82 3.56b 61.00b 64.56b
110–140 0.65 3.46b 13.30b 16.76b
140–180 <LOQ 2.70 ± 0.20 1.00 ± 0.10 3.70 ± 0.30
Taxiway near aircraft hangar Core 5 0–50 <LOQ <LOQ 1.70 ± 0.50 1.70 ± 0.50
50–80 <LOQ <LOQ 3.20 ± 0.34 3.20 ± 0.34
80–110 <LOQ <LOQ 2.50b 2.50b
110–140 <LOQ 3.45b 18.40b 21.85b
140–170 13.50 ± 1.30 148.00 ± 9.70 1201.00 ± 159.00 1349.00 ± 168.70
Driveway Core 6 0–50 5.50 ± 0.40 68.20 ± 1.50 487.00 ± 44.00 555.20 ± 45.50
Near a fire-fighting training pad Core 7 0–50 3.60 ± 0.20 183.00 ± 16.00 1952.00 ± 965.00 2135.00 ± 981.00
50–100 0.92 ± 0.02 <LOQ 2.30 ± 0.40 2.30 ± 0.40


The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.


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