A totally non-ionic pathway to mesoporous Ti-MSU-silicas is reported, wherein the incorporation of Ti into the silica framework proceeds via the hydrolysis of a chemically modified Ti-alkoxide species which permits control over the rate of hydrolysis of the metal precursor, thus allowing stoichiometric titanium incorporation up to approximately 5 mol%.
S. A. Bagshaw, F. Di Renzo and F. Fajula, Chem. Commun., 1996, 2209 DOI: 10.1039/CC9960002209
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