The solubilised septipyridine ligand L is prepared and reacts with zinc(II) acetate to give a head-to-head directional double helicate [Zn2L2][PF6]4·6MeCN which is structurally characterised [space group C2/c, a= 32.845(6), b= 11.979(1), c= 30.244(4)Å, β= 95.79(1)°, R= 0.057].
E. C. Constable, M. Neuburger, D. R. Smith and M. Zehnder, Chem. Commun., 1996, 1917 DOI: 10.1039/CC9960001917
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