A five-step synthesis of O,N-protected (+)-3-deoxynojirimycin (7a) and (+)-3-deoxymannojirimycin (7b) from N-Boc L-serinal acetonide (1) employing 2-acetylthiazole (2) as a masked α-hydroxypropanal β-anion synthon is described.
A. Dondoni, G. Fantin, M. Fogagnolo and P. Merino, J. Chem. Soc., Chem. Commun., 1990, 854 DOI: 10.1039/C39900000854
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